I got two 200gal boxes of Instant Ocean Reef crystals from a fellow member that was getting out of the hobby. They were still sealed and unopened. I used it for my new 90 gal build and there were some leftover particulates that didnt get dissolved and when I turned on my skimmer it was going haywire and bubbling like crazy. I didnt think to much of it. But I made some more water for a water change for my 40gal and the little nano skimmer was overflowing this morning. So does salt go bad? FWIW the salt in the individual bags were semi hard and could be broken up easily by hand.